# assignments file written by GENXPK on Wed Mar 4 10:54:03 PST 1998 #P43M calcium-loaded, pH 6.02 T=300K #assigned from COSY (m34ca11197cy) and NOESY (m34ca11297ny) #fifth column gives assignment status: a = assigned, c = assigned #and confirmed by sequential NOEs, t = tentative assignment, #u = unassigned (value from pH 6.1) #if sixth column for HA resonances is f = completely assigned resiude 1 LYS HA 4.614 c 1 LYS HB+ 1.790 a 1 LYS HB- 1.790 u 1 LYS HD+ 1.750 u 1 LYS HD- 1.750 u 1 LYS HE+ 3.000 a 1 LYS HE- 3.000 u 1 LYS HG+ 1.628 a 1 LYS HG- 1.628 a 1 LYS HN 8.78 c 2 SER HA 4.788 c f 2 SER HB+ 4.446 a 2 SER HB- 4.081 a 2 SER HN 9.046 c 3 PRO HA 4.327 c 3 PRO HB+ 2.485 a 3 PRO HB- 2.021 a 3 PRO HD+ 3.990 a 3 PRO HD- 3.990 a 3 PRO HG+ 2.280 u 3 PRO HG- 2.070 a 4 GLU HA 4.091 a f 4 GLU HB+ 2.102 a 4 GLU HB- 2.016 a 4 GLU HG+ 2.456 a 4 GLU HG- 2.309 a 4 GLU HN 8.771 c 5 GLU HA 4.173 c f 5 GLU HB+ 2.441 a 5 GLU HB- 2.099 a 5 GLU HG+ 2.326 a 5 GLU HG- 2.190 a 5 GLU HN 8.094 c 6 LEU HA 4.267 c f 6 LEU HB+ 2.199 a 6 LEU HB- 1.72 a 6 LEU HG 1.901 a 6 LEU HN 8.565 c 6 LEU MD+ 1.053 a 6 LEU MD- 0.972 a 7 LYS HA 3.982 a 7 LYS HB+ 1.913 a 7 LYS HB- 1.769 a 7 LYS HD+ 1.370 u 7 LYS HD- 1.356 a 7 LYS HE+ 2.685 t 7 LYS HE- 2.640 t 7 LYS HG+ 1.168 a 7 LYS HG- 0.809 a 7 LYS HN 8.283 c 8 GLY HA+ 3.93 a f 8 GLY HA- 3.858 a 8 GLY HN 7.916 c 9 ILE HA 3.891 a f 9 ILE HB 2.21 a 9 ILE HG1+ 1.988 a 9 ILE HG1- 1.217 a 9 ILE HN 8.083 c 9 ILE MD1 0.982 a 9 ILE MG2 1.181 a 10 PHE HA 3.554 c f 10 PHE HB+ 3.34 a 10 PHE HB- 2.694 a 10 PHE HD 6.334 a 10 PHE HE 7.122 a 10 PHE HN 8.483 c 10 PHE HZ 7.637 a 11 GLU HA 3.783 c f 11 GLU HB+ 2.133 a 11 GLU HB- 1.990 a 11 GLU HG+ 2.710 a 11 GLU HG- 2.419 a 11 GLU HN 8.564 c 12 LYS HA 3.855 c 12 LYS HB+ 1.800 u 12 LYS HB- 1.782 a 12 LYS HD+ 1.463 a 12 LYS HD- 1.463 a 12 LYS HE+ 2.766 t 12 LYS HE- 2.750 u 12 LYS HG+ 1.107 a 12 LYS HG- 0.57 a 12 LYS HN 7.740 c 13 TYR HA 4.001 a f 13 TYR HB+ 2.803 a 13 TYR HB- 2.444 a 13 TYR HD 7.433 a 13 TYR HE 6.759 a 13 TYR HN 7.284 c 14 ALA HA 3.803 c f 14 ALA HN 8.369 c 14 ALA MB 0.453 a 15 ALA HA 4.315 a f 15 ALA HN 6.937 c 15 ALA MB 1.439 a 16 LYS HA 3.86 c f 16 LYS HB+ 1.976 a 16 LYS HB- 2.157 a 16 LYS HD+ 1.723 a 16 LYS HD- 1.66 a 16 LYS HE+ 2.955 a 16 LYS HE- 2.739 a 16 LYS HG+ 1.489 a 16 LYS HG- 1.442 a 16 LYS HN 7.17 c 17 GLU HA 4.733 c 17 GLU HB+ 2.020 u 17 GLU HB- 1.920 u 17 GLU HG+ 2.250 a 17 GLU HG- 2.000 u 17 GLU HN 9.659 c 18 GLY HA+ 3.936 a f 18 GLY HA- 3.67 c 18 GLY HN 9.014 c 19 ASP HA 4.698 a f 19 ASP HB+ 2.822 a 19 ASP HB- 2.624 a 19 ASP HN 8.04 c 20 PRO HA 4.793 c 20 PRO HB+ 2.250 a 20 PRO HB- 2.030 a 20 PRO HD+ 3.990 a 20 PRO HD- 3.990 a 20 PRO HG+ 2.076 a 20 PRO HG- 1.930 u 21 ASN HA 4.97 c f 21 ASN HB+ 3.023 a 21 ASN HB- 2.711 a 21 ASN HD2+ 7.946 a 21 ASN HD2- 6.986 a 21 ASN HN 8.984 c 22 GLN HA 5.12 a f 22 GLN HB+ 2.140 a 22 GLN HB- 1.775 a 22 GLN HE2+ 7.475 a 22 GLN HE2- 6.556 a 22 GLN HG+ 2.281 a 22 GLN HG- 2.040 a 22 GLN HN 7.238 c 23 LEU HA 5.496 c f 23 LEU HB+ 2.038 a 23 LEU HB- 1.624 a 23 LEU HG 1.331 a 23 LEU HN 9.536 c 23 LEU MD+ 0.389 a 23 LEU MD- 0.714 a 24 SER HA 4.814 c f 24 SER HB+ 4.380 a 24 SER HB- 4.186 a 24 SER HN 10.056 c 25 LYS HA 3.462 c 25 LYS HB+ 1.315 a 25 LYS HB- 0.445 a 25 LYS HD+ 1.387 a 25 LYS HD- 1.388 a 25 LYS HE+ 2.581 a 25 LYS HE- 2.581 u 25 LYS HG+ 1.038 a 25 LYS HG- 0.664 a 25 LYS HN 8.723 c 26 GLU HA 3.987 c 26 GLU HB+ 1.982 a 26 GLU HB- 1.91 u 26 GLU HG+ 2.359 a 26 GLU HG- 2.234 a 26 GLU HN 8.06 c 27 GLU HA 3.973 c 27 GLU HB+ 2.364 a 27 GLU HB- 1.54 a 27 GLU HG+ 2.450 a 27 GLU HG- 2.27 u 27 GLU HN 7.727 c 28 LEU HA 4.086 a f 28 LEU HB+ 2.33 a 28 LEU HB- 1.554 a 28 LEU HG 1.735 a 28 LEU HN 8.751 c 28 LEU MD+ 1.127 a 28 LEU MD- 1.074 a 29 LYS HA 3.66 c 29 LYS HB+ 2.089 a 29 LYS HB- 1.892 a 29 LYS HD+ 1.649 a 29 LYS HD- 1.649 a 29 LYS HE+ 2.891 a 29 LYS HE- 2.850 u 29 LYS HG+ 1.328 a 29 LYS HG- 1.218 a 29 LYS HN 8.389 c 30 LEU HA 4.035 a f 30 LEU HB+ 1.890 a 30 LEU HB- 1.756 a 30 LEU HG 1.880 a 30 LEU HN 7.649 c 30 LEU MD+ 0.988 a 30 LEU MD- 0.987 a 31 LEU HA 2.336 a f 31 LEU HB+ 1.76 a 31 LEU HB- 1.219 a 31 LEU HG 1.25 a 31 LEU HN 8.162 c 31 LEU MD+ 0.93 a 31 LEU MD- 0.796 a 32 LEU HA 3.883 a f 32 LEU HB+ 2.01 a 32 LEU HB- 1.377 a 32 LEU HG 2.015 a 32 LEU HN 8.79 c 32 LEU MD+ 0.918 a 32 LEU MD- 0.804 a 33 GLN HA 3.859 c f 33 GLN HB+ 2.18 a 33 GLN HB- 1.974 a 33 GLN HE2+ 7.355 a 33 GLN HE2- 6.786 a 33 GLN HG+ 2.527 a 33 GLN HG- 2.379 a 33 GLN HN 8.604 c 34 THR HA 4.07 a f 34 THR HB 4.173 a 34 THR HN 7.604 c 34 THR MG2 1.236 a 35 GLU HA 4.219 c f 35 GLU HB+ 1.323 a 35 GLU HB- 1.475 a 35 GLU HG+ 2.661 a 35 GLU HG- 2.198 a 35 GLU HN 8.386 c 36 PHE HA 5.225 a f 36 PHE HB+ 3.365 a 36 PHE HB- 2.763 a 36 PHE HD 7.138 a 36 PHE HE 7.025 a 36 PHE HN 7.841 c 36 PHE HZ 7.155 a 37 PRO HA 4.206 c f 37 PRO HB+ 2.470 a 37 PRO HB- 1.210 a 37 PRO HD+ 3.523 a 37 PRO HD- 3.102 a 37 PRO HG+ 1.990 a 37 PRO HG- 1.990 a 38 SER HA 4.263 c f 38 SER HB+ 3.996 a 38 SER HB- 3.924 a 38 SER HN 8.413 c 39 LEU HA 4.189 c f 39 LEU HB+ 1.864 a 39 LEU HB- 1.615 a 39 LEU HG 1.702 a 39 LEU HN 7.947 c 39 LEU MD+ 0.937 a 39 LEU MD- 0.763 a 40 LEU HA 4.371 c 40 LEU HB+ 1.80 u 40 LEU HB- 1.701 a 40 LEU HG 1.592 a 40 LEU HN 7.72 c 40 LEU MD+ 0.936 a 40 LEU MD- 0.824 a 41 LYS HA 4.361 c 41 LYS HB+ 1.95 a 41 LYS HB- 1.767 a 41 LYS HD+ 1.682 a 41 LYS HD- 1.682 a 41 LYS HE+ 2.996 a 41 LYS HE- 2.996 a 41 LYS HG+ 1.51 u 41 LYS HG- 1.42 u 41 LYS HN 7.452 c 42 GLY HA+ 4.125 c f 42 GLY HA- 3.981 c 42 GLY HN 8.07 c 43 MET HA 4.453 c f 43 MET HB+ 2.154 a 43 MET HB- 2.063 a 43 MET HG+ 2.643 a 43 MET HG- 2.547 a 43 MET HN 8.315 c 44 SER HA 4.661 c f 44 SER HB+ 4.157 a 44 SER HB- 3.908 a 44 SER HN 8.268 c 45 THR HA 4.418 c f 45 THR HB 4.504 a 45 THR HN 8.012 c 45 THR MG2 1.325 a 46 LEU HA 4.037 a 46 LEU HB+ 1.873 a 46 LEU HB- 1.67 u 46 LEU HG 1.62 u 46 LEU HN 8.669 c 46 LEU MD+ 0.943 a 46 LEU MD- 0.943 a 47 ASP HA 4.198 c f 47 ASP HB+ 2.698 a 47 ASP HB- 2.569 a 47 ASP HN 8.151 c 48 GLU HA 4.045 c f 48 GLU HB+ 2.165 a 48 GLU HB- 2.086 a 48 GLU HG+ 2.35 a 48 GLU HG- 2.35 a 48 GLU HN 7.771 c 49 LEU HA 4.17 c 49 LEU HB+ 1.753 a 49 LEU HB- 1.59 u 49 LEU HG 1.638 a 49 LEU HN 8.345 c 49 LEU MD+ 0.88 u 49 LEU MD- 0.845 a 50 PHE HA 3.664 c 50 PHE HB+ 3.23 a 50 PHE HB- 2.989 a 50 PHE HD 7.131 u 50 PHE HE 7.12 u 50 PHE HN 8.951 c 50 PHE HZ 7.16 u 51 GLU HA 4.00 c f 51 GLU HB+ 2.158 a 51 GLU HB- 2.159 a 51 GLU HG+ 2.545 a 51 GLU HG- 2.372 a 51 GLU HN 7.831 c 52 GLU HA 3.917 c 52 GLU HB+ 2.11 a 52 GLU HB- 2.10 u 52 GLU HG+ 2.28 u 52 GLU HG- 2.03 u 52 GLU HN 7.762 c 53 LEU HA 4.185 c f 53 LEU HB+ 1.663 a 53 LEU HB- 1.141 a 53 LEU HG 2.029 a 53 LEU HN 7.913 c 53 LEU MD+ 0.825 a 53 LEU MD- 0.744 a 54 ASP HA 4.551 c f 54 ASP HB+ 2.542 a 54 ASP HB- 1.605 a 54 ASP HN 7.991 c 55 LYS HA 4.069 c 55 LYS HB+ 1.92 a 55 LYS HB- 1.90 a 55 LYS HD+ 1.749 t 55 LYS HD- 1.747 t 55 LYS HE+ 3.146 t 55 LYS HE- 3.101 t 55 LYS HG+ 1.609 a 55 LYS HG- 1.514 a 55 LYS HN 8.043 c 56 ASN HA 4.838 c f 56 ASN HB+ 3.312 a 56 ASN HB- 2.848 a 56 ASN HD2+ 8.053 a 56 ASN HD2- 6.629 a 56 ASN HN 7.929 c 57 GLY HA+ 3.857 c f 57 GLY HA- 3.857 a 57 GLY HN 7.611 c 58 ASP HA 4.644 c f 58 ASP HB+ 3.152 a 58 ASP HB- 2.466 a 58 ASP HN 8.249 c 59 GLY HA+ 4.271 c f 59 GLY HA- 3.74 c 59 GLY HN 10.515 c 60 GLU HA 5.126 a 60 GLU HB+ 1.903 a 60 GLU HB- 1.513 a 60 GLU HG+ 2.175 a 60 GLU HG- 2.02 u 60 GLU HN 7.802 c 61 VAL HA 5.122 a f 61 VAL HB 2.337 a 61 VAL HN 10.347 c 61 VAL MG+ 1.262 a 61 VAL MG- 0.496 a 62 SER HA 4.879 c f 62 SER HB+ 4.53 a 62 SER HB- 4.201 a 62 SER HG 5.99 a 62 SER HN 9.573 c 63 PHE HA 3.286 c f 63 PHE HB+ 2.655 a 63 PHE HB- 2.461 a 63 PHE HD 6.516 a 63 PHE HE 7.14 a 63 PHE HN 9.612 c 63 PHE HZ 7.361 a 64 GLU HA 3.892 c f 64 GLU HB+ 2.064 a 64 GLU HB- 1.909 a 64 GLU HG+ 2.461 a 64 GLU HG- 2.268 a 64 GLU HN 8.467 c 65 GLU HA 4.084 c f 65 GLU HB+ 1.899 a 65 GLU HB- 1.87 a 65 GLU HG+ 2.556 a 65 GLU HG- 2.369 a 65 GLU HN 7.996 c 66 PHE HA 3.977 c f 66 PHE HB+ 3.29 a 66 PHE HB- 3.131 a 66 PHE HD 6.93 a 66 PHE HE 7.163 a 66 PHE HN 8.878 c 66 PHE HZ 7.111 a 67 GLN HA 3.496 c f 67 GLN HB+ 1.96 a 67 GLN HB- 1.908 a 67 GLN HE2+ 6.169 a 67 GLN HE2- 5.76 a 67 GLN HG+ 2.341 a 67 GLN HG- 2.154 a 67 GLN HN 7.605 c 68 VAL HA 3.577 c f 68 VAL HB 1.945 a 68 VAL HN 7.075 c 68 VAL MG+ 0.839 a 68 VAL MG- 1.034 a 69 LEU HA 3.819 c f 69 LEU HB+ 1.337 a 69 LEU HB- 1.21 a 69 LEU HG 1.278 a 69 LEU HN 7.104 c 69 LEU MD+ 0.724 a 69 LEU MD- 0.61 a 70 VAL HA 3.113 c f 70 VAL HB 1.966 a 70 VAL HN 7.008 c 70 VAL MG+ 0.763 a 70 VAL MG- 0.629 a 71 LYS HA 4.001 c 71 LYS HB+ 1.78 u 71 LYS HB- 1.68 u 71 LYS HD+ 1.608 a 71 LYS HD- 1.608 a 71 LYS HE+ 2.913 a 71 LYS HE- 2.913 a 71 LYS HG+ 1.485 a 71 LYS HG- 1.404 u 71 LYS HN 7.434 c 72 LYS HA 4.138 c f 72 LYS HB+ 1.843 a 72 LYS HB- 1.843 a 72 LYS HD+ 1.473 a 72 LYS HD- 1.473 a 72 LYS HE+ 2.846 a 72 LYS HE- 2.745 a 72 LYS HG+ 1.601 a 72 LYS HG- 1.497 a 72 LYS HN 7.438 c 73 ILE HA 4.03 c f 73 ILE HB 1.744 a 73 ILE HG1+ 1.201 a 73 ILE HG1- 0.735 a 73 ILE HN 7.434 c 73 ILE MD1 0.187 a 73 ILE MG2 0.602 a 74 SER HA 4.515 c f 74 SER HB+ 3.881 a 74 SER HB- 3.882 a 74 SER HN 7.768 c 75 GLN HA 4.168 a 75 GLN HB+ 2.119 a 75 GLN HB- 1.957 a 75 GLN HE2+ 7.51 a 75 GLN HE2- 6.797 a 75 GLN HG+ 2.326 a 75 GLN HG- 2.331 u 75 GLN HN 7.644 c