# assignments file written by GENXPK on Thu Feb 12 11:54:21 PST 1998 #P43M apo, pH 6.01 T=300K #assigned from COSY (m34apo10997cy) and NOESY (m34apo11097ny) #fifth column gives assignment status: a = assigned, c = assigned #and confirmed by sequential NOEs, t = tentative assignment, #u = unassigned (value from pH 5.3) #if sixth column for HA resonances is f = completely assigned resiude 0 MET HA 4.19 a 0 MET HB 2.143 a 0 MET HG 2.665 u 1 LYS HA 4.53 c 1 LYS HB+ 1.87 u 1 LYS HB- 1.735 a 1 LYS HE 2.87 u 2 SER HA 4.756 a f 2 SER HB+ 4.461 a 2 SER HB- 4.097 a 2 SER HN 9.063 c 3 PRO HA 4.326 c 3 PRO HB+ 2.508 a 3 PRO HB- 2.019 t 3 PRO HD 3.99 u 4 GLU HA 4.05 a f 4 GLU HB+ 2.102 a 4 GLU HB- 2.006 a 4 GLU HG+ 2.496 a 4 GLU HG- 2.285 a 4 GLU HN 8.751 c 5 GLU HA 4.175 c 5 GLU HB+ 2.435 a 5 GLU HB- 2.085 a 5 GLU HG+ 2.475 u 5 GLU HG- 2.315 a 5 GLU HN 8.039 c 6 LEU HA 4.327 c f 6 LEU HB+ 2.319 a 6 LEU HB- 1.778 a 6 LEU HG 1.978 a 6 LEU HN 8.799 c 6 LEU MD+ 1.027 a 6 LEU MD- 0.879 a 7 LYS HA 3.762 c f 7 LYS HB+ 1.815 a 7 LYS HB- 1.519 a 7 LYS HD+ 1.208 a 7 LYS HD- 1.091 a 7 LYS HE 2.633 a 7 LYS HG 0.793 a 7 LYS HN 8.528 c 8 GLY QPA 3.95 a f 8 GLY HN 7.773 c 9 ILE HA 3.924 a f 9 ILE HB 2.164 a 9 ILE HG+ 1.995 a 9 ILE HG- 1.236 a 9 ILE HN 7.882 c 9 ILE MD 0.99 a 9 ILE MG 1.153 a 10 PHE HA 3.546 c f 10 PHE HB+ 3.337 a 10 PHE HB- 2.975 a 10 PHE HD 6.509 a 10 PHE HE 7.15 a 10 PHE HN 8.636 c 10 PHE HZ 7.368 a 11 GLU HA 3.89 a f 11 GLU HB+ 2.151 a 11 GLU HB- 2.025 a 11 GLU HG+ 2.66 a 11 GLU HG- 2.412 a 11 GLU HN 8.738 c 12 LYS HA 3.911 c f 12 LYS HB 1.913 a 12 LYS HD+ 1.585 a 12 LYS HD- 1.55 a 12 LYS HE 2.755 a 12 LYS HG+ 1.278 a 12 LYS HG- 0.873 a 12 LYS HN 7.587 c 13 TYR HA 4.041 a f 13 TYR HB+ 2.743 a 13 TYR HB- 2.529 a 13 TYR HD 7.573 a 13 TYR HE 6.721 a 13 TYR HN 7.301 c 14 ALA HA 3.926 a f 14 ALA HN 8.633 c 14 ALA MB 0.691 a 15 ALA HA 4.035 c f 15 ALA HN 7.57 c 15 ALA MB 1.418 a 16 LYS HA 3.846 c f 16 LYS HB+ 1.836 a 16 LYS HB- 1.796 a 16 LYS HD 1.623 a 16 LYS HE 2.812 a 16 LYS HG 1.417 a 16 LYS HN 7.082 c 17 GLU HA 4.481 c f 17 GLU HB+ 2.142 a 17 GLU HB- 1.965 a 17 GLU HG 2.207 a 17 GLU HN 7.425 a 18 GLY HA+ 3.938 c f 18 GLY HA- 3.702 c 18 GLY HN 8.419 c 19 ASP HA 4.80 u 19 ASP HB+ 2.797 a 19 ASP HB- 2.581 u 19 ASP HN 8.588 c 20 PRO HA 4.53 c f 20 PRO HB+ 2.205 a 20 PRO HB- 2.011 a 20 PRO HD 3.867 a 20 PRO HG 1.851 a 21 ASN HA 5.059 c f 21 ASN HB+ 3.005 a 21 ASN HB- 2.805 a 21 ASN HD+ 8.015 a 21 ASN HD- 7.044 a 21 ASN HN 8.789 c 22 GLN HA 5.174 c 22 GLN HB+ 2.062 a 22 GLN HB- 1.765 a 22 GLN HE+ 7.26 a 22 GLN HE- 6.641 a 22 GLN HG+ 2.233 a 22 GLN HG- 2.11 u 22 GLN HN 7.731 c 23 LEU HA 4.81 u 23 LEU HB+ 1.659 t 23 LEU HB- 1.136 a 23 LEU HG 1.375 u 23 LEU HN 8.819 c 23 LEU MD+ 0.517 t 23 LEU MD- 0.455 u 24 SER HA 4.761 c f 24 SER HB+ 4.409 a 24 SER HB- 4.079 a 24 SER HN 8.584 a 25 LYS HA 3.67 c 25 LYS HB+ 1.61 a 25 LYS HB- 1.471 a 25 LYS HE+ 2.809 a 25 LYS HE- 2.706 u 25 LYS HN 8.746 c 26 GLU HA 3.935 a f 26 GLU HB 1.963 a 26 GLU HG+ 2.317 a 26 GLU HG- 2.216 a 26 GLU HN 8.461 c 27 GLU HA 4.07 c 27 GLU HB+ 2.217 a 27 GLU HB- 2.05 u 27 GLU HG+ 2.466 a 27 GLU HG- 2.425 u 27 GLU HN 7.77 c 28 LEU HA 4.01 a f 28 LEU HB+ 2.234 a 28 LEU HB- 1.483 a 28 LEU HG 1.68 a 28 LEU HN 8.686 c 28 LEU MD+ 1.124 a 28 LEU MD- 1.034 a 29 LYS HA 3.743 c 29 LYS HB 1.831 t 29 LYS HD 1.591 a 29 LYS HE 2.909 a 29 LYS HG+ 1.444 a 29 LYS HG- 0.919 a 29 LYS HN 8.188 c 30 LEU HA 4.116 a f 30 LEU HB+ 1.831 a 30 LEU HB- 1.79 a 30 LEU HG 1.73 a 30 LEU HN 7.337 c 30 LEU MD+ 1.028 a 30 LEU MD- 0.977 a 31 LEU HA 3.013 c f 31 LEU HB+ 1.689 a 31 LEU HB- 0.955 a 31 LEU HG 0.983 a 31 LEU HN 8.408 c 31 LEU MD+ 0.905 a 31 LEU MD- 0.489 a 32 LEU HA 4.012 a f 32 LEU HB+ 2.043 a 32 LEU HB- 1.407 a 32 LEU HG 2.052 a 32 LEU HN 8.818 c 32 LEU MD+ 0.84 a 32 LEU MD- 0.756 a 33 GLN HA 4.071 a f 33 GLN HB+ 2.226 a 33 GLN HB- 1.981 a 33 GLN HE+ 7.215 a 33 GLN HE- 6.643 a 33 GLN HG+ 2.552 a 33 GLN HG- 2.377 a 33 GLN HN 8.044 a 34 THR HA 4.069 a f 34 THR HB 4.295 a 34 THR HN 7.931 c 34 THR MG 1.245 a 35 GLU HA 4.255 a f 35 GLU HB+ 1.61 a 35 GLU HB- 1.53 a 35 GLU HG+ 2.503 a 35 GLU HG- 2.217 a 35 GLU HN 8.883 c 36 PHE HA 5.175 a f 36 PHE HB+ 3.345 a 36 PHE HB- 2.975 a 36 PHE HD 7.248 a 36 PHE HE 7.148 a 36 PHE HN 7.822 c 36 PHE HZ 6.993 a 37 PRO HA 4.309 a f 37 PRO HB 2.437 a 37 PRO HD+ 3.523 a 37 PRO HD- 3.231 a 37 PRO HG 1.995 a 38 SER HA 4.338 a f 38 SER HB+ 4.015 a 38 SER HB- 3.936 a 38 SER HN 8.33 c 39 LEU HA 4.38 c f 39 LEU HB+ 1.83 a 39 LEU HB- 1.651 a 39 LEU HG 1.742 a 39 LEU HN 7.877 c 39 LEU MD+ 0.85 a 39 LEU MD- 0.83 a 40 LEU HA 4.329 a 40 LEU HB+ 1.75 a 40 LEU HB- 1.675 u 40 LEU HG 1.736 a 40 LEU HN 7.61 c 40 LEU MD+ 0.92 a 40 LEU MD- 0.826 a 41 LYS HA 4.265 c f 41 LYS HB+ 1.846 a 41 LYS HB- 1.805 a 41 LYS HD 1.687 a 41 LYS HE 3.022 a 41 LYS HG+ 1.456 a 41 LYS HG- 1.412 a 41 LYS HN 7.922 a 42 GLY QPA 4.004 a f 42 GLY HN 8.214 c 43 MET HA 4.478 a f 43 MET HB+ 2.131 a 43 MET HB- 2.084 a 43 MET HG+ 2.703 a 43 MET HG- 2.565 a 43 MET HN 8.192 c 44 SER HA 4.502 c f 44 SER HB+ 4.008 a 44 SER HB- 3.94 a 44 SER HN 8.529 c 45 THR HA 4.336 c f 45 THR HB 4.327 a 45 THR HN 7.778 c 45 THR MG 1.254 a 46 LEU HA 3.997 a f 46 LEU HB+ 1.683 a 46 LEU HB- 1.522 a 46 LEU HG 1.579 a 46 LEU HN 8.182 c 46 LEU MD+ 0.917 a 46 LEU MD- 0.798 a 47 ASP HA 4.255 c f 47 ASP HB+ 2.675 a 47 ASP HB- 2.59 a 47 ASP HN 8.112 a 48 GLU HA 4.067 a f 48 GLU HB+ 2.138 a 48 GLU HB- 2.072 a 48 GLU HG+ 2.357 a 48 GLU HG- 2.171 a 48 GLU HN 7.992 c 49 LEU HA 4.08 c f 49 LEU HB+ 1.73 a 49 LEU HB- 1.529 a 49 LEU HG 1.665 a 49 LEU HN 7.894 c 49 LEU MD+ 0.795 a 49 LEU MD- 0.765 a 50 PHE HA 4.149 a f 50 PHE HB+ 3.26 a 50 PHE HB- 3.158 a 50 PHE HD 7.242 a 50 PHE HE 7.184 a 50 PHE HN 8.408 c 50 PHE HZ 7.056 a 51 GLU HA 4.09 a 51 GLU HB+ 2.208 u 51 GLU HB- 2.136 a 51 GLU HG+ 2.473 u 51 GLU HG- 2.334 a 51 GLU HN 7.824 c 52 GLU HA 4.102 a f 52 GLU HB 2.131 a 52 GLU HG+ 2.379 a 52 GLU HG- 2.242 a 52 GLU HN 7.668 a 53 LEU HA 4.174 c f 53 LEU HB+ 1.663 a 53 LEU HB- 1.495 a 53 LEU HG+ 1.818 a 53 LEU HG- 1.787 a 53 LEU HN 7.658 c 53 LEU MD+ 0.793 a 53 LEU MD- 0.711 a 54 ASP HA 4.515 c 54 ASP HB+ 2.745 a 54 ASP HB- 2.575 u 54 ASP HN 8.201 c 55 LYS HA 4.195 c 55 LYS HB+ 1.904 a 55 LYS HB- 1.749 a 55 LYS HD 1.63 u 55 LYS HE 3.008 a 55 LYS HG+ 1.501 a 55 LYS HG- 1.435 u 55 LYS HN 8.003 c 56 ASN HA 4.761 c 56 ASN HB+ 2.91 a 56 ASN HB- 2.778 u 56 ASN HD+ 7.823 a 56 ASN HD- 6.995 u 56 ASN HN 8.258 c 57 GLY HA+ 4.021 a f 57 GLY HA- 3.944 a 57 GLY HN 8.118 c 58 ASP HA 4.754 a f 58 ASP HB 2.76 a 58 ASP HN 8.405 c 59 GLY HA+ 4.067 a f 59 GLY HA- 3.91 c 59 GLY HN 8.885 a 60 GLU HA 4.916 a f 60 GLU HB+ 1.996 a 60 GLU HB- 1.851 a 60 GLU HG+ 2.308 a 60 GLU HG- 2.137 a 60 GLU HN 7.935 c 61 VAL HA 4.917 c f 61 VAL HB 2.284 a 61 VAL HN 9.146 a 61 VAL MG+ 1.134 a 61 VAL MG- 0.985 a 62 SER HA 5.022 c f 62 SER HB+ 4.522 a 62 SER HB- 4.193 a 62 SER HN 8.626 c 63 PHE HA 3.397 a f 63 PHE HB+ 2.571 a 63 PHE HB- 2.29 a 63 PHE HD 6.59 a 63 PHE HE 7.07 a 63 PHE HN 9.33 c 63 PHE HZ 7.412 a 64 GLU HA 3.707 c f 64 GLU HB+ 2.004 a 64 GLU HB- 1.908 a 64 GLU HG+ 2.368 a 64 GLU HG- 2.222 a 64 GLU HN 8.68 a 65 GLU HA 3.967 c 65 GLU HB+ 2.37 a 65 GLU HB- 2.022 a 65 GLU HN 7.548 c 66 PHE HA 4.125 c f 66 PHE HB+ 3.377 a 66 PHE HB- 3.231 a 66 PHE HD 7.113 a 66 PHE HE 7.335 a 66 PHE HN 8.817 c 66 PHE HZ 7.195 a 67 GLN HA 3.224 c f 67 GLN HB+ 1.727 a 67 GLN HB- 1.722 a 67 GLN HE+ 6.721 a 67 GLN HE- 6.21 a 67 GLN HG 1.647 a 67 GLN HN 8.075 c 68 VAL HA 3.424 c f 68 VAL HB 2.15 a 68 VAL HN 7.117 c 68 VAL MG+ 1.005 a 68 VAL MG- 0.866 a 69 LEU HA 3.889 c f 69 LEU HB+ 1.76 a 69 LEU HB- 1.659 a 69 LEU HG 1.656 a 69 LEU HN 7.741 c 69 LEU MD+ 0.862 a 69 LEU MD- 0.696 a 70 VAL HA 3.082 a f 70 VAL HB 1.445 a 70 VAL HN 7.988 c 70 VAL MG+ 0.402 a 70 VAL MG- 0.028 a 71 LYS HA 3.878 a f 71 LYS HB+ 1.855 a 71 LYS HB- 1.795 a 71 LYS HD 1.66 a 71 LYS HE 2.866 a 71 LYS HG+ 1.46 a 71 LYS HG- 1.328 a 71 LYS HN 7.567 c 72 LYS HA 4.087 a 72 LYS HB 1.928 a 72 LYS HD 1.585 u 72 LYS HE 2.801 a 72 LYS HG+ 1.517 a 72 LYS HG- 1.367 a 72 LYS HN 7.727 a 73 ILE HA 4.333 a f 73 ILE HB 2.025 a 73 ILE HG+ 1.309 a 73 ILE HG- 1.219 a 73 ILE HN 7.52 a 73 ILE MD 0.452 a 73 ILE MG 0.811 a 74 SER HA 4.504 a f 74 SER HB+ 3.865 a 74 SER HB- 3.823 a 74 SER HN 7.524 a 75 GLN HA 4.128 a 75 GLN HB+ 2.137 a 75 GLN HB- 1.95 a 75 GLN HE+ 7.50 a 75 GLN HE- 6.795 a 75 GLN HG 2.34 a 75 GLN HN 7.535 a