# masterlist.2
#
# update of masterlist.orig (=masterlist.sort) after evaluation of bcp182ny
#
#$1 = assignment; $2 = frequency; $3 = dim. in which freq. was measured;
#$4 = experiment in which measurement was made; $5 = region of spectrum in
#which frequency measurement was made; $6 = other comments
mo1          incomplete; a, b ambig; g unknown; e tentative                
m01ha  4.23  w2 bcp035ty  w2=alpha  tentative; see alt shift=4.45 
m01ha  4.45  w2 gsc29d2q  w2=alpha  dxpk; not confirmed; see alt.shift=4.23
m01hb1 2.15  w1 bcp035ty  w2=alpha tentative; see alternative; see alt. shift=2.32
m01hb1 2.32  w1 gsc29d2q  w2=alpha  dxpk; not confirmed; see alt. shift=2.15
m01hb2 2.52  w1 bcp035ty  w2=alpha tentative; see alternative; see alt. shift=2.57
m01hb2 2.57  w1 gsc29d2q  w2=alpha  weak dxpk; not confirmed; see alt. shift=2.52
m01he  2.03  w1 bcp182ny  w2=amide assigned via corr'n to ala02
a02ha  4.459 w1 bcp212rc  w2=methyl 
a02ha  4.461 w1 bcp212rc  w2=amide
a02hb  1.417 w2 bcp212rc  w2=methyl
a02hn  8.389 w2 bcp212rc  w2=amide
s03ha  4.876 w1 bcp212rc  w2=amide
s03hb1 4.05  w1 bcp035ty  w2=amide
s03hb2 4.53  w1 bcp035ty  w2=amide
s03hb2 4.55  w2 d20       w2=alpha
s03hn  9.298 w2 bcp212rc  w2=amide
p04          incomplete: g2
p04ha  4.38  w2 gsc29d2q  w2=alpha dxpk
p04hb1 1.95  w1 gsc29d2q  w2=alpha dxpk
p04hb2 2.52  w1 gsc29d2q  w2=alpha dxpk
p04hd1 3.99  w2 bcp035ty  w2=alpha
p04hd2 4.22  w2 bcp035ty  w2=alpha
p04hg1 2.34  w1 bcp035ty  w2=alpha
l05ha  4.125 w1 bcp212rc  w2=amide 
l05hb1 1.644 w1 bcp162ty  w2=amide nh/b xpks line up poorly
l05hb2 1.765 w1 bcp162ty  w2=amide nh/b xpks line up poorly
l05hd1 0.958 w2 bcp212rc  w2=methyl
l05hd2 0.82  w2 gsc27dcy  w2=methyl
l05hg  1.726 w1 bcp212rc  w2=methyl
l05hn  8.939 w2 bcp162ty  w2=amide nh/b xpks line up poorly
l05hn  8.942 w2 bcp162ty  w2=amide nh/b xpks line up poorly
l05hn  8.942 w2 bcp212rc  w2=amide
d06ha  4.247 w1 bcp212rc  w2=amide
d06hb1 2.70  w1 gsc29d2q  w2=alpha rxpk
d06hb2 3.08  w1 gsc29d2q  w2=alpha dxpk
d06hn  7.991 w2 bcp212rc  w2=amide
q07ha  4.072 w1 bcp212rc  w2=amide
q07hb1 2.14  w1 gsc29d2q  w2=alpha rxpk
q07hb2 2.261 w1 bcp162ty  w2=amide
q07hg  2.461 w1 bcp172ty  w2=amide weak xpk
q07hn  8.595 w2 bcp212rc  w2=amide
q07hs1 7.143 w2 bcp182ny w2=arom
q07hs2 6.796 w2 bcp182ny w2=arom
a08ha  4.089 w1 bcp212rc  w2=amide  
a08hb  1.685 w2 bcp212rc  w2=methyl
a08hn  8.485 w2 bcp212rc  w2=amide
a08hn  8.487 w2 bcp212rc  w2=amide
i09ha  3.733 w1 bcp212rc  w2=amide  
i09hb  2.115 w1 bcp212rc  w2=methyl
i09hd  0.811 w2 bcp212rc  w2=methyl
i09hg1 0.879 w2 bcp212rc  w2=methyl
i09hg2 1.294 w1 bcp212rc  w2=methyl
i09hg3 1.722 w1 bcp212rc  w2=methyl
i09hn  8.492 w2 bcp212rc  w2=amide
g10ha1 3.943 w1 bcp212rc  w2=amide see noesy shift=3.989
g10ha1 3.989 best fit for bcp182ny
g10ha1 3.992 w1 gsc27dcy  w2=amide see noesy shift=3.989
g10ha2 3.740 best fit for bcp182ny
g10ha2 3.76  w1 gsc29d2q  w2=amide rxpk; see noesy shift=3.740
g10hn  8.308 w2 bcp212rc  w2=amide 8.3075 182ny
l11ha  4.303 w1 bcp212rc  w2=amide crowded region/overlap
l11hb1 1.473 w1 bcp192dr  w2=methyl
l11hb2 2.18  w1 gsc29d2q  w2=alpha dxpk
l11hd1 0.968 w2 bcp212rc  w2=methyl
l11hd2 0.970 w2 bcp192dr  w2=methyl
l11hg  1.892 w1 bcp212rc  w2=methyl
l11hn  8.252 w2 bcp212rc  w2=amide crowded region/overlap   
l12ha  4.069 w1 bcp212rc  w2=amide
l12hb1 1.539 w1 bcp172ty  w2=amide weak xpk
l12hb2 2.46  w1 gsc29d2q  w2=alpha dxpk
l12hd1 0.721 w2 bcp212rc  w2=methyl
l12hd2 0.770 w2 bcp212rc  w2=methyl
l12hg  1.970 w1 bcp212rc  w2=methyl
l12hn  8.226 w2 bcp212rc  w2=amide
i13ha  3.604 w1 bcp212rc  w2=amide  
i13hb  1.795 w1 bcp212rc  w2=methyl
i13hd  0.392 w2 bcp212rc  w2=methyl
i13hg1 0.493 w2 bcp212rc  w2=methyl
i13hg2 0.049 w1 bcp212rc  w2=methyl
i13hg3 1.742 w1 bcp212rc  w2=methyl
i13hn  8.739 w2 bcp212rc  w2=amide see noesy shift=8.746
i13hn  8.746 best fit for noesy 
g14ha1 4.134 w1 gsc27dcy  w2=amide see alt. shift=4.148
g14ha1 4.148 w1 bcp162ty  w2=amide see alt. shift=4.134
g14ha2 3.94  w1 gsc29d2q  w2=amide rxpk 
g14hn  8.352 w2 bcp162ty  w2=amide
i15ha  3.990 w1 bcp212rc  w2=amide 
i15hb  2.105 w1 bcp212rc  w2=methyl
i15hd  0.904 w2 bcp212rc  w2=methyl
i15hg1 1.157 w2 bcp212rc  w2=methyl
i15hg2 1.603 w1 bcp212rc  w2=methyl
i15hg3 1.677 w1 bcp212rc  w2=methyl
i15hn  8.259 w2 bcp212rc  w2=amide
f16ha  3.644 w1 gsc27dcy  w2=amide
f16hb1 2.877 best fit for noesy
f16hb1 2.93  w1 bcp2162q  w2=alpha rxpk; see noesy H2O shift=2.877
f16hb2 3.179 best fit for noesy
f16hb2 3.21  w1 bcp2162q  w2=alpha dxpk; see noesy H2O shift=3.179
f16hd  6.126 w2 bcp212rc  w2=arom 
f16he  7.001 w2 bcp212rc  w2=arom
f16hf  7.343 w2 bcp212rc  w2=arom 
f16hn  7.622 w2 gsc27dcy  w2=amide see noesy shift=7.631
f16hn  7.631 best fit for noesy
h17          incomplete; ring protons
h17ha  4.91  w1 gsc29d2q  w2=amide dxpk; see noesy shift=4.873
h17ha  4.87  w1 bcp182ny  w2=amide see alt. shift=4.91
h17hb  3.20  w1 bcp035ty  w2=amide see alt. shift=3.17
h17hb  3.17  w1 bcp182ny  w2=amide see alt. shift=3.20
h17hn  8.60  w2 gsc29d2q  w2=amide dxpk; see noesy shift=8.607
h17hn  8.607 bcp182ny
h17hr1 7.224 bcp182ny
k18          incomplete
k18ha  3.940 w1 bcp212rc  w2=amide degen with a79  
k18hb1 1.98  w1 bcp035ty  w2=amide weak xpk
k18hb2 2.17  w1 bcp035ty  w2=amide
k18hn  8.021 w2 bcp212rc  w2=amide degen with a79
y19ha  4.195 w1 bcp212rc  w2=amide 
y19hb1 2.520 w1 bcp212rc  w2=amide
y19hb2 2.932 w1 bcp162ty  w2=amide
y19hd  7.544 w2 bcp212rc  w2=arom 
y19he  6.767 w2 bcp212rc  w2=arom 
y19hn  7.206 w2 bcp212rc  w2=amide
s20          incomplete: hn 
s20ha  4.76  w2 d20       w2=alpha
s20hb1 3.80  w2 d20       w2=alpha
s20hb2 3.91  w2 d20       w2=alpha 
g21ha1 3.778 w1 gsc27dcy  w2=amide 
g21ha2 4.00  w1 gsc29d2q  w2=amide remote xpk
g21hn  8.020 w2 gsc27dcy  w2=amide
k22          incomplete
k22h   1.36  w1 bcp035ty  w2=amide
k22h   1.46  w1 bcp035ty  w2=amide
k22h   1.59  w1 bcp035ty  w2=amide
k22h   1.67  w1 bcp035ty  w2=amide weak xpk
k22ha  4.082 w1 bcp172ty  w2=amide see alt. shifts
k22ha  4.086 w1 bcp212rc  w2=amide see alt. shifts
k22ha  4.088 w1 bcp162ty  w2=amide see alt. shifts
k22hb1 1.79  w1 gsc29d2q  w2=alpha dxpk
k22hb2 1.82  w1 gsc29d2q  w2=alpha rxpk
k22hn  7.696 w2 bcp212rc  w2=amide
e23ha  4.406 w1 bcp212rc  w2=amide
e23hb1 1.896 w1 bcp212rc  w2=amide
e23hb2 2.070 w1 bcp192dr  w2=amide
e23hg  2.186 w1 bcp162ty  w2=amide
e23hn  8.126 w2 bcp212rc  w2=amide
g24ha1 3.724 w1 gsc27dcy  w2=amide see alt. shift=3.742
g24ha1 3.742 w1 bcp192dr  w2=amide see alt. shift=3.724
g24ha2 3.94  w1 gsc29d2q  w2=amide remote xpk
g24hn  8.306 w2 gsc27dcy  w2=amide see alt. shift=8.310
g24hn  8.310 w2 bcp192dr  w2=amide see alt. shift=8.306
d25ha  4.507 w1 bcp212rc  w2=amide 
d25hb1 2.601 w1 bcp192dr  w2=amide
d25hb2 2.846 w1 bcp212rc  w2=amide
d25hn  8.342 w2 bcp212rc  w2=amide
k26          incomplete  
k26ha  4.230 w1 bcp212rc  w2=amide
k26hn  8.227 w2 bcp212rc  w2=amide
h27          incomplete; ring protons
h27ha  5.008 w1 bcp212rc  w2=amide
h27hb1 3.31  w2 gsc29d2q  w2=alpha dxpk
h27hb1 3.315 bcp182ny
h27hb2 3.47  w2 gsc29d2q  w2=alpha dxpk
h27hb2 3.476 bcp182ny
h27hn  8.872 w2 bcp212rc  w2=amide
h27hr  7.253 bcp182ny
t28ha  5.235 w1 bcp212rc  w2=amide  
t28hb  4.141 w1 bcp212rc  w2=methyl
t28hg  1.072 w2 bcp212rc  w2=methyl
t28hn  7.616 w2 bcp212rc  w2=amide
l29ha  4.800 w1 bcp212rc  w2=amide
l29hb1 1.290 w1 bcp162ty  w2=amide
l29hb2 1.491 w1 bcp162ty  w2=amide
l29hd1 0.497 w2 bcp212rc  w2=methyl
l29hd2 0.544 w2 bcp212rc  w2=methyl
l29hg  1.359 w1 bcp212rc  w2=methyl
l29hn  8.670 w2 bcp212rc  w2=amide
s30          incomplete; betas
s30ha  5.145 w1 bcp212rc  w2=amide
s30hb1 4.03     noesy     tentative
s30hb2 4.43     noesy     tentative
s30hn  8.885 w2 bcp212rc  w2=amide
k31          incomplete
k31ha  3.806 w1 gsc27dcy  w2=amide
k31hb1 1.58  w1 bcp2162q  w2=alpha dxpk
k31hb2 1.66  w1 bcp2162q  w2=alpha rxpk  
k31hn  8.574 w2 gsc27dcy  w2=amide
k32          incomplete
k32ha  4.109 w1 bcp212rc  w2=amide
k32hb1 1.83  w1 bcp035ty  w2=amide
k32hn  8.516 w2 bcp212rc  w2=amide
e33ha  4.172 w1 bcp212rc  w2=amide
e33hb1 2.11  w1 gsc29d2q  w2=alpha rxpk
e33hb2 2.40  w1 gsc29d2q  w2=alpha dxpk
e33hg  2.34  w1 bcp035ty  w2=alpha
e33hn  7.682 w2 bcp212rc  w2=amide
l34ha  3.944 w1 bcp212rc  w2=amide
l34hb1 1.20  w1 bcp035ty  w2=methyl
l34hb2 2.10  w1 gsc29d2q  w2=alpha dxpk
l34hd1 0.417 w2 bcp212rc  w2=methyl
l34hd2 1.062 w2 bcp212rc  w2=methyl
l34hg  1.299 w1 bcp212rc  w2=methyl
l34hn  8.559 w2 bcp212rc  w2=amide
k35          incomplete
k35ha  3.556 w1 bcp212rc  w2=amide
k35hb1 1.74  w1 gsc29d2q  w2=alpha rxpk
k35hb2 2.07  w1 gsc29d2q  w2=alpha dxpk
k35hn  8.015 w2 bcp212rc  w2=amide
e36ha  3.979 w1 bcp212rc  w2=amide
e36hb  2.179 w1 bcp162ty  w2=amide degen betas
e36hg1 2.349 w1 bcp172ty  w2=amide
e36hg2 2.441 w1 bcp172ty  w2=amide
e36hn  7.221 w2 bcp212rc  w2=amide
e36hn  7.223 w2 bcp162ty  w2=amide
l37ha  3.071 w1 bcp212rc  w2=amide
l37ha  3.086 w1 bcp162ty  w2=amide
l37hb1 0.88  w1 bcp035ty  w2=alpha
l37hb2 1.58  w1 bcp035ty  w2=alpha
l37hd1 0.689 w2 bcp212rc  w2=methyl
l37hd2 0.731 w2 bcp212rc  w2=methyl
l37hg  1.225 w1 bcp212rc  w2=methyl
l37hn  8.158 w2 bcp212rc  w2=amide
i38ha  3.361 w1 bcp212rc  w2=amide  
i38hb  1.977 w1 bcp212rc  w2=methyl
i38hd  0.787 w2 bcp212rc  w2=methyl
i38hg1 0.853 w2 bcp212rc  w2=methyl
i38hg2 1.432 w1 bcp212rc  w2=methyl
i38hg3 1.608 w1 bcp212rc  w2=methyl
i38hn  8.200 w2 bcp212rc  w2=amide
q39ha  3.964 w1 bcp212rc  w2=amide
q39hb1 2.02  w1 gsc29d2q  w2=alpha rxpk
q39hb2 2.241 w1 bcp162ty  w2=amide
q39hg  2.66  w1 bcp234ty  w2=amide ~pH6.2
q39hn  7.926 w2 bcp212rc  w2=amide
q39hs1 7.169 w2 bcp182ny  w2=arom
q39hs2 6.842 w2 bcp182ny  w2=arom
k40          incomplete 
k40h   1.17  w1 bcp234ty  w2=amide
k40h   1.50  w1 bcp234ty  w2=amide
k40h   1.53  w1 bcp035ty  w2=amide
k40h   1.61  w1 bcp234ty  w2=amide
k40h   1.62  w1 bcp035ty  w2=amide
k40h   1.67  w1 bcp234ty  w2=amide
k40h   1.71  w1 bcp035ty  w2=amide
k40h   1.79  w1 bcp234ty  w2=amide
k40h   1.80  w1 bcp035ty  w2=amide weak xpk
k40ha  4.339 w1 bcp212rc  w2=amide
k40hb1 1.894 w1 bcp162ty  w2=amide weak xpk
k40hb2 2.105 w1 bcp212rc  w2=amide
k40hn  8.271 w2 bcp212rc  w2=amide see alt. shifts
k40hn  8.273 w2 bcp212rc  w2=amide see alt. shifts
k40hn  8.276 w2 bcp162ty  w2=amide weak xpk; see alt. shifts
e41          incomplete; g
e41ha  4.689 w1 bcp212rc  w2=amide
e41hb1 1.836 w1 bcp212rc  w2=amide
e41hb2 2.41  w1 bcp035ty  w2=amide see alt. shift in d20=2.42
e41hb2 2.42  w1 bcp2162q  w2=alpha rxpk; see alt. shift@310=2.41
e41hn  8.528 w2 bcp212rc  w2=amide
l42ha  4.76  w1 gsc29d2q  w2=amide dxpk
l42hb1 1.922 w1 bcp212rc  w2=amide
l42hb2 1.60  w1 bcp035ty  w2=amide
l42hd1 0.740 w2 bcp212rc  w2=methyl
l42hd2 0.841 w2 bcp212rc  w2=methyl
l42hg  1.301 w1 bcp212rc  w2=methyl
l42hn  7.837 w2 bcp212rc  w2=amide
t43ha  4.294 w1 bcp212rc  w2=amide degen with t43hb          
t43hb  4.294 w1 bcp212rc  w2=methyl degen with t43ha
t43hg  1.176 w2 bcp212rc  w2=methyl 
t43hn  9.858 w2 bcp162ty  w2=amide see alt. shift=9.862
t43hn  9.862 w2 bcp212rc  w2=amide see alt. shift=9.858
i44ha  3.797 w1 bcp212rc  w2=amide crowded region/overlap; see alt. shift=3.807
i44ha  3.807 w1 bcp162ty  w2=amide see potential alt. shift=3.797 
i44hb  1.543 w1 bcp212rc  w2=amide,methyl
i44hd  0.446 w2 bcp212rc  w2=methyl
i44hg1 0.442 w2 bcp212rc  w2=methyl
i44hg2 0.446 w2 bcp212rc  w2=methyl
i44hg3 1.105 w1 bcp212rc  w2=methyl
i44hn  7.924 w2 bcp212rc  w2=amide
g45ha1 3.726 w1 gsc27dcy  w2=amide 
g45ha2 4.01  w1 gsc29d2q  w2=amide remote xpk
g45hn  8.439 w2 gsc27dcy  w2=amide
s46          incomplete:  nh freq at pH7 
s46ha  4.31  w2 gsc29d2q  w2=alpha dxpk  
s46hb1 3.95  w2 gsc29d2q  w2=alpha dxpk
s46hb2 4.04  w2 gsc29d2q  w2=alpha dxpk
s46hn  8.81  w2 bcp093ty  w2=amide pH6.2; titrating?
k47          incomplete 
k47h   1.53  w1 bcp035ty  w2=alpha
k47h   1.60  w1 bcp035ty  w2=alpha
k47ha  4.329 w1 bcp212rc  w2=amide
k47hb1 1.770 w1 bcp212rc  w2=amide
k47hb2 1.94  w1 gsc29d2q  w2=alpha rxpk
k47he  3.065 w1 bcp172ty  w2=amide weak xpk; see alt shift@310=3.08
k47he  3.08  w1 bcp035ty  w2=alpha see alt. shift=3.065 
k47hn  7.864 w2 bcp212rc  w2=amide
l48ha  3.997 w1 bcp212rc  w2=amide 
l48hb1 1.578 w1 bcp162ty  w2=amide weak xpk
l48hb2 1.658 w1 bcp162ty  w2=amide
l48hd1 0.826 w2 bcp212rc  w2=methyl
l48hd2 0.924 w2 bcp212rc  w2=methyl
l48hg  1.688 w1 bcp212rc  w2=methyl
l48hn  7.604 w2 bcp212rc  w2=amide
q49ha  4.270 w1 bcp212rc  w2=amide
q49hb1 1.95  w1 gsc29d2q  w2=alpha dxpk
q49hb2 2.323 w1 bcp162ty  w2=amide
q49hg  2.61  w1 bcp035ty  w2=alpha weak xpk;?
q49hn  7.512 w2 bcp212rc  w2=amide
q49hn  7.514 w2 bcp162ty  w2=amide
q49hs1 7.455 w2 bcp182ny  w2=arom
q49hs2 6.770 w2 bcp182ny  w2=arom
d50ha  4.408 w1 bcp212rc  w2=amide 
d50hb1 2.754 w1 bcp162ty  w2=amide degen betas
d50hb2 2.754 w1 bcp162ty  w2=amide degen betas 
d50hn  7.739 w2 bcp162ty  w2=amide
d50hn  7.742 w2 bcp212rc  w2=amide
a51ha  3.960 w1 bcp212rc  w2=methyl 
a51hb  1.484 w2 bcp212rc  w2=methyl
a51hn  8.890 w2 bcp212rc  w2=amide
e52ha  4.125 w1 bcp212rc  w2=amide degen with l05  
e52hb  2.078 w1 bcp162ty  w2=amide see alt shifts=2.09,2.06
e52hb1 2.09  w1 gsc29d2q  w2=alpha dxpk; see alt. shifts
e52hb2 2.06  w1 gsc29d2q  w2=alpha rxpk; see alt. shifts
e52hg1 2.33  w1 bcp035ty  w2=alpha
e52hg2 2.42  w1 bcp035ty  w2=alpha
e52hn  8.942 w2 bcp212rc  w2=amide degen with l05
i53ha  3.769 w1 bcp212rc  w2=amide   
i53hb  2.260 w1 bcp212rc  w2=amide
i53hd  0.856 w2 bcp212rc  w2=methyl
i53hg1 0.908 w2 bcp212rc  w2=methyl
i53hg2 1.146 w1 bcp212rc  w2=methyl
i53hg3 1.762 w1 bcp212rc  w2=methyl
i53hn  7.516 w2 bcp212rc  w2=amide
v54ha  3.494 w1 bcp212rc  w2=amide  
v54hb  1.981 w1 bcp212rc  w2=methyl
v54hg1 0.917 w2 bcp212rc  w2=methyl
v54hg2 0.963 w2 bcp212rc  w2=methyl
v54hn  8.470 w2 bcp212rc  w2=amide
k55          incomplete
k55h   1.445 w1 bcp172ty  w2=amide weak xpk
k55h   1.73  w1 bcp035ty  w2=k-epsilon
k55ha  4.093 w1 bcp212rc  w2=amide
k55hb1 1.876 w1 bcp212rc  w2=amide
k55hb2 1.83  w1 bcp2162q  w2=alpha ambiguous assignment
k55he  2.98  w2 bcp035ty  w2=k-epsilon
k55hn  7.518 w2 bcp212rc  w2=amide see alt. shift=7.522
k55hn  7.522 w2 bcp172ty  w2=amide weak xpk; see alt. shift=7.518
l56ha  4.226 w1 bcp212rc  w2=amide crowded region/overlap  
l56hb1 1.938 w1 bcp212rc  w2=amide
l56hb2 1.61  w1 gsc29d2q  w2=alpha rxpk
l56hd1 0.690 w2 bcp212rc  w2=methyl
l56hd2 0.730 w2 bcp212rc  w2=methyl
l56hg  1.795 w1 bcp212rc  w2=methyl
l56hn  7.264 w2 bcp212rc  w2=amide
m57          incomplete; Me 
m57ha  4.330 w1 bcp212rc  w2=amide
m57hb1 2.332 w1 bcp162ty  w2=amide
m57hb2 2.00  w1 gsc29d2q  w2=alpha rxpk
m57hg1 2.68  w1 bcp035ty  w2=alpha
m57hg2 2.83  w1 bcp035ty  w2=alpha
m57hn  8.508 w2 bcp212rc  w2=amide
d58ha  4.431 w1 bcp212rc  w2=amide 
d58hb1 2.65  w1 gsc29d2q  w2=alpha rxpk
d58hb2 2.860 w1 bcp212rc  w2=amide
d58hn  8.797 w2 bcp212rc  w2=amide
d58hn  8.799 w2 bcp212rc  w2=amide
d59ha  4.336 w1 bcp212rc  w2=amide 
d59hb1 2.821 w1 bcp162ty  w2=amide
d59hb2 2.898 w1 bcp162ty  w2=amide weak xpk
d59hn  7.581 w2 bcp212rc  w2=amide see alt. shifts
d59hn  7.583 w2 bcp162ty  w2=amide see alt. shifts
d59hn  7.585 w2 bcp162ty  w2=amide weak xpk; see alt. shifts
l60ha  3.928 w1 bcp212rc  w2=amide 
l60hb1 2.03  w1 bcp2262qf w2=alpha
l60hb2 1.48  w1 bcp035ty  w2=methyl
l60hd1 0.475 w2 bcp212rc  w2=methyl
l60hd2 0.710 w2 bcp212rc  w2=methyl
l60hg  2.030 w1 bcp212rc  w2=methyl
l60hn  7.562 w2 bcp212rc  w2=amide
d61ha  4.487 w1 bcp212rc  w2=amide 
d61hb  2.738 w1 bcp162ty  w2=amide betas degen @ pH7?	
d61hb1 2.78  w1 bcp2162q  w2=alpha dxpk shifted in d2o?
d61hb2 2.70  w1 bcp2162q  w2=alpha rxpk shifted in d2o?
d61hn  7.329 w2 bcp212rc  w2=amide
r62ha  4.103 w1 bcp212rc  w2=amide 
r62hb1 1.853 w1 bcp212rc  w2=amide
r62hb2 1.87  w1 gsc29d2q  w2=alpha rxpk
r62hd  3.233 w1 bcp162ty  w2=amide see alt. shift=3.242
r62hd  3.242 w1 bcp172ty  w2=amide see alt. shift=3.233
r62he  7.419 w2 bcp162ty  w2=amide
r62hg1 1.629 w1 bcp172ty  w2=amide
r62hg2 1.759 w1 bcp172ty  w2=amide 
r62hn  8.083 w2 bcp212rc  w2=amide see alt. shifts
r62hn  8.085 w2 bcp212rc  w2=amide see alt. shifts
r62hn  8.087 w2 bcp172ty  w2=amide see alt. shifts
r62hn  8.092 w2 bcp172ty  w2=amide see alt. shifts
n63ha  5.118 w1 bcp212rc  w2=amide
n63hb1 2.523 w1 bcp162ty  w2=amide nh chem shift?
n63hb2 3.01  w1 gsc29d2q  w2=alpha rxpk
n63hn  7.838 w2 bcp212rc  w2=amide 
n63hs1 7.669 w2 bcp182ny  w2=arom
n63hs2 6.900 w2 bcp182ny  w2=arom
d65ha  4.835 w1 bcp212rc  w2=amide
d65hb1 2.589 w1 bcp212rc  w2=amide
d65hb2 2.844 w1 bcp192dr  w2=amide
d65hn  8.308 w2 bcp212rc  w2=amide
q66ha  4.168 w1 bcp212rc  w2=amide
q66hb  2.078 w1 bcp212rc  w2=amide betas degen
q66hg1 2.416 w1 bcp162ty  w2=amide
q66hg2 2.553 w1 bcp162ty  w2=amide
q66hn  7.982 w2 bcp212rc  w2=amide
q66hs1 7.704 w2 bcp182ny  w2=arom
q66hs2 6.835 w2 bcp182ny  w2=arom
e67ha  4.689 w1 bcp212rc  w2=amide degen with e41; see alt. shift=4.752  
e67ha  4.752 w1 bcp172ty  w2=amide weak xpk; see alt. shift=4.689
e67hb1 1.88  w2 bcp2162q  w2=alpha rxpk
e67hb2 1.928 w1 bcp172ty  w2=amide
e67hg1 2.13  w1 bcp035ty  w2=amide
e67hg2 2.316 w1 bcp172ty  w2=amide
e67hn  8.513 w2 bcp172ty  w2=amide see alt. shift=8.528
e67hn  8.528 w2 bcp212rc  w2=amide degen with e41; see alt. shift=8.513
v68ha  4.704 w1 gsc27dcy  w2=amide 
v68hb  2.229 w1 bcp212rc  w2=methyl
v68hg1 0.823 w2 bcp212rc  w2=methyl
v68hg2 0.885 w2 bcp212rc  w2=methyl see alt. shift=.891
v68hg2 0.891 w1 bcp162ty  w2=amide see alt. shift=.885
v68hn  9.408 w2 bcp212rc  w2=amide 
n69ha  5.286 w1 bcp212rc  w2=amide
n69hb1 3.00  w1 bcp035ty  w2=amide
n69hb2 3.637 best fit for noesy
n69hb2 3.65  w1 bcp035ty  w2=amide see noesy shift=3.637
n69hn  8.907 w2 bcp212rc  w2=amide
n69hs1 7.462 w2 bcp182ny  w2=arom
n69hs2 7.112 w2 bcp182ny  w2=arom
f70ha  3.27  w2 gsc29d2q  w2=alpha dxpk
f70ha  3.281 w1 bcp212rc  w2=amide wk/skewed; occurs where "expected" from ny nh/a xpk; real?
f70hb1 2.44  w1 gsc29d2q  w2=alpha rxpk
f70hb2 2.64  w1 gsc29d2q  w2=alpha dxpk
f70hd  6.358 w2 bcp212rc  w2=arom  
f70he  6.912 w2 bcp212rc  w2=arom
f70hf  6.833 best fit for noesy?
f70hf  6.841 w2 bcp212rc  w2=arom see noesy shift=6.833?
f70hn  9.125 w2 bcp212rc  w2=amide wk/skewed; occurs where "expected" from ny nh/a xpk; real?
q71ha  3.677 w1 bcp212rc  w2=amide
q71hb1 2.20  w1 gsc29d2q  w2=alpha dxpk
q71hb2 2.00  w1 gsc29d2q  w2=alpha rxpk
q71hg  2.27  w1 bcp093ty  w2=amide
q71hn  7.670 w2 bcp212rc  w2=amide
q71hs1 7.161 w2 bcp182ny  w2=arom
q71hs2 7.023 w2 bcp182ny  w2=arom
e72ha  3.926 w1 bcp212rc  w2=amide
e72hb1 2.36  w1 gsc29d2q  w2=alpha dxpk
e72hb2 1.95  w1 gsc29d2q  w2=alpha rxpk
e72hg1 2.27  w1 bcp035ty  w2=alpha
e72hg2 2.51  w1 bcp035ty  w2=alpha
e72hn  8.550 w2 bcp212rc  w2=amide
y73ha  4.243 w1 bcp212rc  w2=amide 
y73hb1 3.06  w1 bcp2463q  w1=beta
y73hb2 3.12  w2 bcp2463q  w1=beta
y73hd  6.717 w2 bcp212rc  w2=arom 
y73he  6.538 w2 bcp212rc  w2=arom   
y73hn  8.484 w2 bcp212rc  w2=amide
i74ha  3.155 w1 bcp212rc  w2=amide  
i74hb  1.287 w1 bcp212rc  w2=methyl
i74hd  0.407 w2 bcp212rc  w2=methyl
i74hg1 0.590 w2 bcp212rc  w2=methyl
i74hg2 0.794 w1 bcp212rc  w2=methyl
i74hg3 0.917 w1 bcp212rc  w2=methyl
i74hn  8.037 w2 bcp212rc  w2=amide
t75ha  3.576 w1 bcp212rc  w2=amide  
t75hb  4.148 w1 bcp212rc  w2=methyl
t75hg  1.182 w2 bcp212rc  w2=methyl 
t75hn  8.121 w2 bcp212rc  w2=amide
t75hn  8.123 w2 bcp172ty  w2=amide 
f76ha  4.115 w1 bcp212rc  w2=amide
f76hb1 3.24  w1 gsc29d2q  w2=alpha dxpk
f76hb2 3.17  w1 gsc29d2q  w2=alpha rxpk 
f76hd  7.112 w2 bcp212rc  w2=arom 
f76he  7.245 w2 bcp212rc  w2=arom 
f76hf  7.089 w2 bcp212rc  w2=arom overlapped peak  
f76hn  7.949 w2 bcp212rc  w2=amide
l77ha  3.869 w1 bcp212rc  w2=amide crowded region/overlap  
l77hb1 1.078 w1 bcp192dr  w2=methyl
l77hb2 1.86  w2 gsc29d2q  w2=alpha dxpk
l77hd1 0.378 w2 bcp212rc  w2=methyl
l77hd2 0.694 w2 bcp212rc  w2=methyl
l77hg  1.621 w1 bcp212rc  w2=methyl
l77hn  7.971 w2 bcp212rc  w2=amide crowded region/overlap
g78ha1 3.530 w1 bcp162ty  w2=amide see alt. shifts 
g78ha1 3.538 w1 gsc27dcy  w2=amide see alt. shifts
g78ha1 3.559 w1 bcp172ty  w2=amide weak xpk; see alt. shifts
g78ha2 3.676 w1 gsc27dcy  w2=amide
g78hn  8.377 w2 bcp162ty  w2=amide best fit for noesy
a79ha  3.940 w1 bcp212rc  w2=amide  
a79hb  1.316 w2 bcp212rc  w2=methyl
a79hn  8.021 w2 bcp212rc  w2=amide
a79hn  8.024 w2 bcp212rc  w2=amide
l80ha  3.818 w1 bcp212rc  w2=amide 
l80hb1 1.72  w1 gsc29d2q  w2=alpha dxpk
l80hb2 1.49  w1 gsc29d2q  w2=alpha rxpk
l80hd1 0.735 w2 bcp212rc  w2=methyl
l80hd2 0.806 w2 bcp212rc  w2=methyl
l80hg  1.528 w1 bcp212rc  w2=methyl
l80hn  7.973 w2 bcp212rc  w2=amide
a81ha  3.573 w1 bcp212rc  w2=amide,methyl  
a81hb  1.213 w2 bcp212rc  w2=methyl 
a81hn  8.638 w2 bcp212rc  w2=amide see alt. shift=8.642
a81hn  8.642 w2 bcp162ty  w2=amide see alt. shift=8.638
m82          incomplete; Me
m82ha  3.841 w1 bcp212rc  w2=amide
m82hb1 2.13  w1 gsc29d2q  w2=alpha dxpk
m82hb2 2.14  w1 gsc29d2q  w2=alpha dxpk
m82hg1 2.55  w1 bcp035ty  w2=alpha
m82hg2 2.9   w1 bcp035ty  w2=alpha
m82hn  7.494 w2 bcp212rc  w2=amide
i83ha  3.941 w1 bcp212rc  w2=amide  
i83hb  1.883 w1 bcp212rc  w2=methyl
i83hd  0.738 w2 bcp212rc  w2=methyl
i83hg1 0.814 w2 bcp212rc  w2=methyl
i83hg2 1.035 w1 bcp212rc  w2=methyl
i83hg3 1.631 w1 bcp212rc  w2=methyl
i83hn  7.367 w2 bcp212rc  w2=amide
y84ha  4.674 w1 bcp212rc  w2=amide
y84hb1 3.22  w2 gsc29d2q  w2=alpha dxpk
y84hb2 2.53  w1 gsc29d2q  w2=alpha dxpk
y84hd  6.956 w2 bcp212rc  w2=arom 
y84he  6.675 w2 bcp212rc  w2=arom   
y84hn  7.905 w2 bcp212rc  w2=amide
n85ha  4.296 w1 bcp162ty  w2=amide 
n85hb  2.51  w1 gsc29d2q  w2=alpha dxpk degen betas
n85hn  7.761 w2 bcp162ty  w2=amide 
n85hs1 6.930 w2 bcp182ny  w2=arom
n85hs2 6.480 w2 bcp182ny  w2=arom
e86ha  3.851 w1 bcp212rc  w2=amide 
e86hb1 2.01  w1 gsc29d2q  w2=alpha dxpk
e86hb2 2.09  w1 gsc29d2q  w2=alpha rxpk
e86hg1 2.33  w1 bcp093ty  w2=alpha
e86hg2 2.39  w1 bcp093ty  w2=alpha
e86hn  9.073 w2 bcp212rc  w2=amide
a87ha  4.253 w1 bcp212rc  w2=amide  
a87hb  1.409 w2 bcp212rc  w2=methyl
a87hn  8.273 w2 bcp212rc  w2=amide
l88ha  4.289 w1 bcp212rc  w2=amide 
l88hb1 1.492 w1 bcp212rc  w2=amide
l88hb2 1.576 w1 bcp192dr  w2=methyl
l88hb2 1.579 w1 bcp192dr  w2=methyl
l88hd1 -.057 w2 bcp212rc  w2=methyl
l88hd2 0.326 w2 bcp212rc  w2=methyl
l88hg  0.961 w1 bcp212rc  w2=methyl
l88hn  7.416 w2 bcp212rc  w2=amide
k89          incomplete
k89h   1.373 w1 bcp162ty  w2=amide
k89h   1.409 w1 bcp162ty  w2=amide
k89h   1.612 w1 bcp162ty  w2=amide
k89ha  4.265 w1 bcp212rc  w2=amide
k89hb1 1.745 w1 bcp212rc  w2=amide
k89hb2 1.841 w1 bcp212rc  w2=amide
k89he  2.924 w1 bcp162ty  w2=amide
k89hn  7.274 w2 bcp212rc  w2=amide see alt. shift=7.278
k89hn  7.278 w2 bcp162ty  w2=amide see alt. shift=7.274
g90ha1 3.733 w1 bcp212rc  w2=amide
g90ha2 3.733 w1 bcp212rc  w2=amide
g90hn  7.919 w2 bcp212rc  w2=amide
qnX1   7.651 H17hr2?
qnX2   6.539 H17hr3?